مجلة جامعة تشرين للبحوث والدراسات العلمية، سلسلة العلوم الأساسية (Dec 2019)

Synthesis of C16H14PSNO3 and determination of some of its physical properties and extraction capacity of vanadium ions (V) and nickel (II) from their aqueous media

  • معين نعمان,
  • فيصل أحمد

Journal volume & issue
Vol. 41, no. 6

Abstract

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The ortho-chrysol-oxy-quinolines ThiO-hydroxy-phosphate or phosphorous was formulated with the chemical formula C16H14PSNO3 to be used as a solvent extract of nickel (II) and vanadium (V) ions from their aqueous media. The identification of the compound was determined using IR spectroscopy and some physical properties (melting point, color and appearance) were determined. The ratio of some elements in the prepared compound: sulfur, phosphorus and carbon was determined according to the methods mentioned in the international references UOP and ASTM and Some factors influencing the extraction process, such as stirring time, were investigated to achieve the equilibrium and concentration associated with the organic phase, the pH effect and the water-to-organic ratio. The percentage of extraction and the extraction constant were also calculated.