IUCrData (Jan 2017)

1-Ethyl-4-phenyl-1,5-benzodiazepine-2-thione

  • Lhoussaine El Ghayati,
  • Noureddine Hamou Ahabchane,
  • Mohamadou Lamine Doumbia,
  • Nada Kheira Sebbar,
  • El Mokhtar Essassi,
  • Joel T. Mague

DOI
https://doi.org/10.1107/S2414314616019982
Journal volume & issue
Vol. 2, no. 1
p. x161998

Abstract

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In the title compound, C17H16N2S, the seven-membered ring adopts a boat conformation. The two aromatic rings are inclined at an angle of 34.7 (1)° to one another. The molecules pack in helical chains running along the c-axis direction through C—H...S hydrogen bonds. These are further linked into layers parallel to (100) by weak C—H...π(ring) interactions. The structure was refined as a two-component inversion twin.

Keywords