Processing and Application of Ceramics (Sep 2016)

Synthesis of silver doped hydroxyapatite nanospheres using Ouzo effect

  • Marija Prekajski,
  • Bojan Jokić,
  • Ana Kalijadis,
  • Jelena Maletaškić,
  • Nadežda Stanković,
  • Jelena Luković,
  • Branko Matović

DOI
https://doi.org/10.2298/PAC1603169P
Journal volume & issue
Vol. 10, no. 3
pp. 169 – 174

Abstract

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Nanoemulsion technique, based on Ouzo effect, was applied for synthesis of the pure and silver doped (2.5 and 5 mol%) calcium hydroxyapatite (HAp). After calcination at 500 °C fully crystallized powders were obtained. X-ray powder diffraction analysis accompanied with Rietveld refinement revealed that the synthesized powders were single-phase hydroxyapatite. Raman spectroscopy also confirmed that the synthesized powders were single-phase. The obtained HAp particles were spherical in shape and their sizes were in the nanometer range which was revealed by field emission scanning electron microscopy analysis (FESEM). The successful synthesis of the single-phase Ag doped HAp showed that nanoemulsion method is a simple technique for obtaining pure and doped hydroxyapatite nanospheres.

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