Quantitative Microstructure Prediction of Powder High-Temperature Alloy during Solution Heat Treatment and Its Validation

Abstract

Heat treatment, particularly solution heat treatment, is a critical process in the preparation of powder metallurgy superalloys, where the cooling process significantly impacts the microstructure. This study, based on thermodynamic and kinetic databases as well as the precipitation mechanism of strengthening phases, delves into the influence of cooling process, especially the cooling path, on the material’s microstructure. The results indicate that under slow cooling rates, the precipitated phases are more likely to exhibit a multimodal size distribution, while under rapid cooling rates, a unimodal distribution may form. The average cooling rate does not consistently accurately reflect the growth of the precipitated phases; even with the same average cooling rate, different cooling paths can lead to significant differences in the size of the precipitates. To accurately predict the size of the precipitates, it is necessary to consider the specific cooling process. Constant cooling rate experiments designed for the study and the dissection testing of full-size turbine discs produced in manufacturing validated the calculated results of the precipitates. Therefore, optimizing cooling through simulation calculations can effectively and accurately control the precipitates, thereby obtaining a microstructure that can meet performance requirements.

Keywords

• solution heat treatment
• cooling path
• calculations
• powder metallurgy superalloy