Regioselective synthesis and crystal structure of ethyl-4-acetyl-5-((2- ethoxy-2-oxoethyl)thio)-3-hydroxythiophene-2-carboxylate, C13H16O6S2

Mabkhot Y. N.; Al-Showiman S. S.; Barakat A.; Yousuf S.; Choudhary M. I.

doi:10.1515/ncrs-2015-0007

Zeitschrift für Kristallographie - New Crystal Structures (Sep 2015)

Regioselective synthesis and crystal structure of ethyl-4-acetyl-5-((2- ethoxy-2-oxoethyl)thio)-3-hydroxythiophene-2-carboxylate, C13H16O6S2

Mabkhot Y. N.,
Al-Showiman S. S.,
Barakat A.,
Yousuf S.,
Choudhary M. I.

Affiliations

Mabkhot Y. N.: Department of Chemistry, College of Science, King Saud University, P. O. Box 2455, Riyadh-11451, Saudi Arabia
Al-Showiman S. S.: Department of Chemistry, College of Science, King Saud University, P. O. Box 2455, Riyadh-11451, Saudi Arabia
Barakat A.: Department of Chemistry, College of Science, King Saud University, P. O. Box 2455, Riyadh-11451, Saudi Arabia
Yousuf S.: H.E.J. Research Institute of Chemistry, International Center for Chemical Sciences, University of Karachi, Karachi-75270, Pakistan
Choudhary M. I.: Department of Chemistry, College of Science, King Saud University, P. O. Box 2455, Riyadh-11451, Saudi Arabia

DOI: https://doi.org/10.1515/ncrs-2015-0007
Journal volume & issue: Vol. 230, no. 3
pp. 241 – 242

Abstract

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C13H16O6S2, triclinic, P1̅ (no. 2), a = 7.979(1) Å, b = 9.189(1) Å, c = 10.263(1) Å, ɑ = 72.876(2)°, β = 71.485(2)°, γ = 76.655(2)°, V = 674.0 Å3, Z = 2, Rgt(F) = 0.0360, wRref(F2) = 0.0962, T = 273 K.

Published in Zeitschrift für Kristallographie - New Crystal Structures

ISSN: 1433-7266 (Print); 2197-4578 (Online)
Publisher: De Gruyter
Country of publisher: Germany
LCC subjects: Science: Physics; Science: Chemistry: Crystallography
Website: https://www.degruyter.com/journal/key/ncrs/html

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