Study of kinetical laws of process of the catalytic synthesis of nanocarbon from methane

Abstract

In the study, the kinetic laws of the process of catalytic synthesis of nanoglyceum from methane were studied in the presence of a catalyst containing Fe2(MoO4)3*MoO3/HSZ. The catalyst containing Fe2(MoO4)3*MoO3/HSZ was prepared by hydrothermal processing. An Empyrean, Malvern Panalytical (Germany) X-ray Diffractometer (XRD) equipped with a modern computer was used to perform X-ray analysis of the samples. The phase composition of the nanocarbon was analyzed using a semi-quantitative method using X-ray diffractograms. The morphology and structure of the product using electron illumination microscopy (accelerating voltage of 40 to 120 kV, cathode-tungsten) in a microscope brand JEM-1400 (JEOL, Japan), were also examined using a scanning electron microscope brand JSM-7001F (JEOL). At a linear velocity of 20 cm/min of gas and a mass of 10 mg of catalyst, the effect of temperature on the synthesis of nanocarbons in the Fe2(MoO4)3*MoO3catalyst was investigated. The work aims to study the kinetic laws of the process of catalytic synthesis of nanocarbon from methane and some characteristics of the resulting product and catalyst.

Keywords

• methane
• nanocarbon
• catalyst
• yield
• catalyst layer height
• texture characteristic
• diffractogram