Molbank (Jan 2023)
2-{9-(10-Bromoanthracenyl)}-1,3-dihydro-1<i>H</i>-[<i>d</i>]-1,3,2-benzodiazaborole
Abstract
In this paper, a synthesis and characterization of a novel three coordinate 2-{9-(10-Bromoanthracenyl)}-1,3-dihydro-1H-[d]-1,3,2-benzodiazaborole from a cyclo-condensation reaction of o-phenylenediamine and 10-bromoanthracene-9-boronic acid is described. The desired product was obtained in 0.343 g (92% yields) with its structure characterized by 1H, 11B, 13C NMR, HRMS and FT-IR.
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