Sensors (Jan 2024)

Optrode-Assisted Multiparametric Near-Infrared Spectroscopy for the Analysis of Liquids

  • Maria Giulia Delli Santi,
  • Salvatore Castrignano,
  • Marialuisa Capezzuto,
  • Marco Consales,
  • Patrizio Vaiano,
  • Andrea Cusano,
  • Gianluca Gagliardi,
  • Pietro Malara

DOI
https://doi.org/10.3390/s24030729
Journal volume & issue
Vol. 24, no. 3
p. 729

Abstract

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We demonstrate a sensing scheme for liquid analytes that integrates multiple optical fiber sensors in a near-infrared spectrometer. With a simple optofluidic method, a broadband radiation is encoded in a time-domain interferogram and distributed to different sensing units that interrogate the sample simultaneously; the spectral readout of each unit is extracted from its output signal by a Fourier transform routine. The proposed method allows performing a multiparametric analysis of liquid samples in a compact setup where the radiation source, measurement units, and spectral readout are all integrated in a robust telecom optical fiber. An experimental validation is provided by combining a plasmonic nanostructured fiber probe and a transmission cuvette in the setup and demonstrating the simultaneous measurement of the absorption spectrum and the refractive index of water–methanol solutions.

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