Физико-химические аспекты изучения кластеров, наноструктур и наноматериалов (Dec 2021)
ANALYSIS OF METHODS FOR STUDYING THE SIZE OF NANOPARTICLES
Abstract
In the presented work, various methods for determining the size of nanoparticles are considered. An effective method for finding possible options has been determined. Information on various methods and studies was selected and analyzed. Fundamentally different methods for finding the sizes of nanoparticles are considered. Non-contact (optical) methods are the most promising. The particle size ranges of the investigated particles are analyzed and presented using the next methods: optical microscopy, electron microscopy, scanning probe microscopy. The principles of operation and possible schemes of installations for studying the material under study are described. The sedimentation method, using centrifugation and the X-ray principle of detection, is described in more detail. Its advantages over other methods are noted. Examples are given of its use in an experimental setup that allows obtaining differential and integral characteristics in various bases, which make it possible to analyze the particle size distribution in the granulometric study of materials, including nanomaterials.
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