Case Studies in Chemical and Environmental Engineering (Dec 2024)

Comparing two synthesis methods: Exploring unique characteristics and catalytic activity of fenton catalyst Fe3O4/zeolite-NaY in methylene blue degradation

  • Dinia Astira,
  • Romario Abdullah,
  • Utari Zulfiani,
  • Dety Oktavia Sulistiono,
  • Zeni Rahmawati,
  • Triyanda Gunawan,
  • Mohd Hafiz Dzarfan Othman,
  • Muhammad Hasan,
  • Ratna Ediati,
  • Hamzah Fansuri

Journal volume & issue
Vol. 10
p. 100963

Abstract

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A composite catalyst was developed to degrade methylene blue (MB) via the Fenton reaction from Fe3O4 and H2O2 with zeolite-NaY as magnetite support to reduce agglomeration. Hydrothermal and co-precipitation approaches were used to synthesize the composite. The co-precipitation method here was proven to be more suitable to produce the composite. Under optimal conditions, all composite catalysts achieved a remarkable MB reduction (more than 90 %) as confirmed through TLC analysis and UV–Vis spectra. Notably, based on linear regression, FeZ-A maintained over 60 % activity after 15 uses, while FeZ-2 showed the least Fe ion leaching. This demonstrated the effectiveness and stability of the developed catalysts.

Keywords