Effect of Heat Treatment on Microstructure and Properties of 24CrNiMo Alloy Steel Formed by Selective Laser Melting (SLM)

Abstract

The 24CrNiMo alloy steel powder was used as experimental material. The microstructure and mechanical properties of as-deposited, quenched and tempered (QT) and stress-relief annealed (SR) specimens were analyzed. The X-ray diffraction (XRD) analysis showed that the specimens in the three states were mainly ferrite (α-Fe), in which the as-deposited samples had puny face-centered cubic (FCC) structure Fe (γ-Fe). The microstructure observation showed that the as-deposited specimens were made up of ferrite, granular bainite, a small amount of cementite and residual austenite. The tensile test results indicated that the tensile strength and yield strength of the as-deposited specimens were 1199 MPa and 1053 MPa respectively, and the elongation at break was 10.7%. The elongation of QT and SR specimens increased to 11.6% and 12.8%, respectively. The electron backscattered scattering detection (EBSD) analysis results showed that the small-angle grain boundary content of the as-deposited samples was 58%, and large-angle grain boundary content was 15%. After QT and SR, small-angle and large-angle grain boundaries were obtained than those in the as-deposited specimens. The high-temperature friction and wear properties and thermal fatigue performances of the QT and SR specimens were improved significantly. The QT specimens had the smallest wear and thermal fatigue crack lengths, excellent resistance to friction and wear performance and prevention of crack growth, with an ideal comprehensive properties.

Keywords

• 24CrNiMo alloy steel powder
• SLM
• heat treatment
• thermal fatigue
• grain orientation