Materials Research (Oct 2015)

Synthesis of SnSb2Te4 Microplatelets by High-energy Ball Milling

  • Mário Sérgio da Luz,
  • Fernando Pacheco Tofanello,
  • Murilo Senhuki Esposto,
  • Ariana de Campos,
  • Bento Ferreira,
  • Carlos Alberto Moreira dos Santos

DOI
https://doi.org/10.1590/1516-1439.359114
Journal volume & issue
Vol. 18, no. 5
pp. 953 – 956

Abstract

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AbstractIn this work we demonstrate that high-energy ball milling process can be used to synthesize SnSb2Te4 without surfactant and further annealing. Milling parameters such as ball to raw material ratio (5:1) and milling time (2h) were determined to be suitable for synthesizing microplatelets of SnSb2Te4. The powders after milling for various durations were characterized by X-ray powder diffraction, scanning electron microscopy and electrical resistance measurements.

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