Dynamic precipitation and dynamic recrystallization behaviors of Mg-Gd-Nd-Zr magnesium alloy during thermal compression deformation

Abstract

In this paper, the dynamic precipitation and dynamic recrystallization (DRX) behaviors of Mg-7Gd-2Nd-0.5Zr (wt.%) alloy during thermal compression were investigated by optical microscopy (OM), scanning electron microscope (SEM) and transmission electron microscopy (TEM). The hot compression tests were performed at 350–500 °C with strain rates of 0.003–1 s−1 and a strain of 0.7. The results indicate that dynamic precipitation and DRX occur in the deformed region under appropriate conditions, and that dynamic precipitation precedes DRX. Elevated deformation temperature and strain rate facilitate DRX but weaken dynamic precipitation. The dynamic precipitates were β (Mg5Gd) phases and were mainly located at the grain boundaries in the deformed regions. DRX can be promoted when the size of the granular precipitates is larger than 200 nm. The second phase particles located at the grain boundaries of the recrystallized grains can pin the grain boundaries to refine the recrystallized grains. There are three mechanisms of recrystallization nucleation: grain boundary bowing nucleation, dislocation pile-up induced nucleation, and particle-stimulated nucleation (PSN). Moreover, a critical strain model and a kinetic model for the DRX of the alloy were developed.

Keywords

• Mg-7Gd-2Nd-0.5Zr alloy
• Thermal compression
• Dynamic precipitation
• Dynamic recrystallization