Acta Crystallographica Section E (Aug 2009)

7,7-Dimethyl-3,3,4a-tris(3-methylbut-2-enyl)-4a,5,6,7-tetrahydro-2H-chromene-2,4(3H)-dione

  • Katrin Möws,
  • Markus Schürmann,
  • Hans Preut,
  • Bernd Plietker

DOI
https://doi.org/10.1107/S1600536809025021
Journal volume & issue
Vol. 65, no. 8
pp. o1751 – o1751

Abstract

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The title compound, C26H38O3, was prepared by an intramolecular Claisen-like cyclization of ethyl 2-acetoxy-4,4-dimethyl-1-(3-methylbut-2-enyl)cyclohex-2-enecarboxylate followed by dialkylation. One of the methyl groups is disordered over two sets of sites in a 0.67:0.33 ratio.