Acta Crystallographica Section E (Dec 2012)

9-(5-Bromo-1H-indol-3-yl)-1,2,3,4,5,6,7,8,9,10-decahydroacridine-1,8-dione dimethyl sulfoxide monosolvate

  • Ahmed El-Khouly,
  • Sema Öztürk Yildirim,
  • Ray J. Butcher,
  • Rahime Şimsek,
  • Cihat Şafak

DOI
https://doi.org/10.1107/S1600536812045886
Journal volume & issue
Vol. 68, no. 12
pp. o3337 – o3337

Abstract

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In the title compound, C21H19BrN2O2·C2H6OS, the indole ring system is essentially planar, with a maximum deviation of 0.050 (3) Å for the non-bridgehead C atom adjacent to the N atom. The two cyclohex-2-enone rings adopt half-chair conformations. An intramolecular C—H...O hydrogen bond occurs. The solvent molecule exhibits minor disorder of the S atom [site occupancies = 0.8153 (16) and 0.1847 (18)]. In the crystal, molecules are linked by N—H...O hydrogen bonds, forming layers parallel to the bc plane.