Determination of Constitutive Equation and Thermo–Mechanical Processing Map for Pure Iridium

Abstract

Deformation behavior of pure iridium has been studied during thermal compression testing with the help of Gleeble-1500D in the temperature range of 1200 °C~1500 °C and strain rate range of 10−1 s−1~10−2 s−1. Resistance to deformation, microstructural evolution and hot workability of pure iridium have been used to analyze in detail. Frictional coefficient has been used to modify the experimental stress–strain curve of thermal compression test, and it has been found effective in reducing the influence of friction during thermo–mechanical testing. The hyperbolic sine constitutive equation of pure iridium has been established to give a material processing model for numerical simulation. A very high value of activation energy for iridium, 573 KJ/mol, clearly indicates that it is very hard to deform this material. The deformation mechanism of pure iridium is dependent upon temperature as well as strain rate. At low temperature and strain rate (temperature range of 1200 °C~1300 °C and strain rate range of 10−1 s−1~10−2 s−1), dynamic recovery is active while dynamic recrystallization becomes operative as temperature and stain rate are increased. On further increase in temperature and decrease in strain rate (temperature range of 1400 °C~1500 °C and strain rates of 10−2 s−1~10−3 s−1), abnormal grain growth takes place. On the basis of a constitutive model and processing map, suitable forming process parameters (temperature range of 1400 °C~1500 °C and strain rate range of 0.1 s−1~0.05 s−1) for pure iridium have been worked out.

Keywords

• hot compression test
• constitutive equation
• microstructural evolution
• deformation mechanisms
• processing maps