Acta Crystallographica Section E (Feb 2008)

2-Anilino-3-benzoyl-4-(2,5-dichlorophenyl)-7,7-dimethyl-5-oxo-5,6,7,8-tetrahydro-4H-benzo[b]pyran

  • Huai-Yuan Xie,
  • Chen Ji,
  • Ji-Hui Sun,
  • Li-Rong Wen

DOI
https://doi.org/10.1107/S1600536807068377
Journal volume & issue
Vol. 64, no. 2
pp. o407 – o407

Abstract

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The title compound, C30H25Cl2NO3, was prepared by the reaction of 3-oxo-N,3-diphenylpropanethioamide, 2,5-dichlorobenzaldehyde and 5,5-dimethyl-1,3-cyclohexanedione (1:1:1) in ethanol. The cyclohexene ring adopts a half-chair conformation. The crystal structure exhibits intramolecular N—H...O and C—H...O, and intermolecular C—H...O interactions.