Acta Crystallographica Section E: Crystallographic Communications (Apr 2015)

Crystal structure of diethyl 3,3′-{2,2′-(1E)-[1,4-phenylenebis(azan-1-yl-1-ylidene)]bis(methan-1-yl-1-ylidene)bis(1H-pyrrole-2,1-diyl)}dipropanoate

  • Jasim Alshawi,
  • Muoayed Yousif,
  • Gregore Timco,
  • Inigo J. Vitorica Yrezabal,
  • Richard Winpenny,
  • Mohamad J. Al-Jeboori

DOI
https://doi.org/10.1107/S2056989015005113
Journal volume & issue
Vol. 71, no. 4
pp. o259 – o260

Abstract

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The complete molecule of the title compound, C26H30N4O4, is generated by crystallographic inversion symmetry. The dihedral angle between the planes of the benzene and pyrrole rings is 45.20 (11)°; the N atom bonded to the the benzene ring and the pyrrole N atom are in a syn conformation. The side chain adopts an extended conformation [N—C—C—C = 169.07 (17)° and C—O—C—C = −176.54 (17)°]. No directional interactions could be identified in the crystal packing.

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