Synthesis and crystallographic characterization of 6-hydroxy-1,2-dihydropyridin-2-one

Sara K. Phillips; Savannah G. Brancato; Samantha N. MacMillan; Mark J. Snider; Andrew J. Roering; Katherine A. Hicks

doi:10.1107/S205698902300974X

Acta Crystallographica Section E: Crystallographic Communications (Dec 2023)

Synthesis and crystallographic characterization of 6-hydroxy-1,2-dihydropyridin-2-one

Sara K. Phillips,
Savannah G. Brancato,
Samantha N. MacMillan,
Mark J. Snider,
Andrew J. Roering,
Katherine A. Hicks

Affiliations

Sara K. Phillips: Department of Chemistry, The State University of New York at Cortland, Cortland, New York 13045, USA
Savannah G. Brancato: Department of Chemistry, The State University of New York at Cortland, Cortland, New York 13045, USA
Samantha N. MacMillan: Department of Chemistry and Chemical Biology, Cornell University, Ithaca, New York 14853, USA
Mark J. Snider: Department of Chemistry, The College of Wooster, Wooster, Ohio 44691, USA
Andrew J. Roering: Department of Chemistry, The State University of New York at Cortland, Cortland, New York 13045, USA
Katherine A. Hicks: Department of Chemistry, The State University of New York at Cortland, Cortland, New York 13045, USA

DOI: https://doi.org/10.1107/S205698902300974X
Journal volume & issue: Vol. 79, no. 12
pp. 1147 – 1150

Abstract

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The title compound, C5H5NO2, is a hydroxylated pyridine ring that has been studied for its involvement in microbial degradation of nicotinic acid. Here we describe its synthesis as a formic acid salt, rather than the standard hydrochloride salt that is commercially available, and its spectroscopic and crystallographic characterization.

Published in Acta Crystallographica Section E: Crystallographic Communications

ISSN: 2056-9890 (Online)
Publisher: International Union of Crystallography
Country of publisher: United Kingdom
LCC subjects: Science: Chemistry: Crystallography
Website: https://journals.iucr.org/e/

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