مجلة التربية والعلم (Dec 2013)

Ultrasound Assisted Synthesis Of Pyrazolone Derivatives

  • Badie Ahmed,
  • Jasim Abdullah

DOI
https://doi.org/10.33899/edusj.2013.163055
Journal volume & issue
Vol. 26, no. 5
pp. 57 – 63

Abstract

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ABSTRACT The diazonium salt of 4-amino-1,5-dimethyl-2-phenyl-1H-pyrazol- 2-one (4-aminoantipyrine) was coupled with ethylacetoacetate and ethyl benzoylacetate to give the corresponding diazo compounds under basic media. These products were allowed to react with hydrazine hydrate and phenylhydrazine under Ultrasound method to give pyrazolone derivatives (I) in high yields.

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