IUCrJ (Sep 2017)

Coherent amplification of X-ray scattering from meso-structures

  • Julien R. Lhermitte,
  • Aaron Stein,
  • Cheng Tian,
  • Yugang Zhang,
  • Lutz Wiegart,
  • Andrei Fluerasu,
  • Oleg Gang,
  • Kevin G. Yager

DOI
https://doi.org/10.1107/S2052252517008107
Journal volume & issue
Vol. 4, no. 5
pp. 604 – 613

Abstract

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Small-angle X-ray scattering (SAXS) often includes an unwanted background, which increases the required measurement time to resolve the sample structure. This is undesirable in all experiments, and may make measurement of dynamic or radiation-sensitive samples impossible. Here, we demonstrate a new technique, applicable when the scattering signal is background-dominated, which reduces the requisite exposure time. Our method consists of exploiting coherent interference between a sample with a designed strongly scattering `amplifier'. A modified angular correlation function is used to extract the symmetry of the interference term; that is, the scattering arising from the interference between the amplifier and the sample. This enables reconstruction of the sample's symmetry, despite the sample scattering itself being well below the intensity of background scattering. Thus, coherent amplification is used to generate a strong scattering term (well above background), from which sample scattering is inferred. We validate this method using lithographically defined test samples.

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