Crystals (Nov 2021)
The Influence of Ni-Added Fe-Based Pre-Alloy on Microstructure Evolution and Lifetime Extension of Diamond Tools
Abstract
Diamond tools were prepared by sintering Fe-Cu-Sn-Zn-Ni pre-alloyed powders and diamonds. The effects of Ni contents in pre-alloyed powders on microstructure evolution of Fe-based matrix, the properties of Fe-based matrix and the service life of diamond tools were investigated. The results showed that adding 3~15 wt.% Ni into the Fe-Cu-Sn-Zn pre-alloyed powders refined the microstructure of the Fe-based matrix and improved its density and hardness gradually. The addition of Ni reduced the loss of low melting liquid phase at a low sintered temperature, thus resulting in a decrease of the pores, an increase of the density and hardness of Fe-based matrix. When the Ni content is less than 9 wt.%, the bending strength of Fe-based matrix and diamond tools, together with the holding force of Fe-based matrix to diamonds increases sharply. They reached up to the optimal value with the Ni content of 9 wt.%. At this sintering powder ratio, the sufficient Fe-Cu-Sn-Zn-Ni liquid phase had a good wettability on the surface of diamonds, thus the optimal performance of sintered matrix and diamond tools was obtained. The service life of diamond tools was prolonged greatly owing to the excellent bonding capacity between matrix and diamonds. Once the Ni content exceeded 9 wt.%, the corresponding value decreased gradually. The fracture morphologies of the matrix changed from the brittle fracture into brittle-ductile fracture, then ductile fracture (with the Ni content of 9 wt.%), brittle-ductile mixed fracture and brittle fracture.
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