Molecules (Apr 2019)

Optimization of Spray-Drying Process of <i>Jerusalem artichoke</i> Extract for Inulin Production

  • Zhenzhou Zhu,
  • Mailing Wu,
  • Jie Cai,
  • Shuyi Li,
  • Krystian Marszałek,
  • Jose M. Lorenzo,
  • Francisco J. Barba

DOI
https://doi.org/10.3390/molecules24091674
Journal volume & issue
Vol. 24, no. 9
p. 1674

Abstract

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Jerusalem artichoke is an important natural matrix for inulin production. In this experiment, response surface methodology (RSM) was employed to optimize the spray-drying parameters in order to determine the maximal inulin yield. For this study, three independent variables (heating temperature (Tª, 110−120 °C), creep speed (V, 18−22 rpm) and pressure (P, 0.02−0.04 MPa)) were used in the experimental design. Using the Box−Behnken design, the optimal parameters obtained were: drying temperature 114.6 °C, creep speed 20.02 rpm, and pressure: 0.03 MPa. The inulin yield, water content and particle size of inulin obtained by spray-drying and freeze-drying were compared. In this regard, the spray-dried inulin consisted of a white powder having a fine particle size, and the freeze-dried inulin had a pale-yellow fluffy floc. On the other hand, the drying methods had a great influence on the appearance and internal structure of inulin powder, since the spray-dried inulin had a complete and uniform shape and size, whereas the freeze-dried inulin had a flocculated sheet structure. The analysis showed that the spray-drying led to a higher inulin yield, lower water content and better surface structure than freeze-drying.

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