Science of Sintering (Jan 2021)

Facile co-precipitation route for magnesium ferrites nanostructure: Synthesis, influence of pH variation on structural properties

  • Gole Devi A.,
  • Kapatkar S.B.,
  • Mathad Shridhar N.,
  • Chavan Rakesh R.

DOI
https://doi.org/10.2298/SOS2101067G
Journal volume & issue
Vol. 53, no. 1
pp. 67 – 78

Abstract

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This report presents the synthesis of magnesium ferrite (MgFe2O4) by coprecipitation method and its subsequent characterization by using X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FTIR) techniques. XRD results confirm the formation of single phase cubic spinel structure, having lattice constant from 8.3216 Å to 8.3252 Å. An infrared spectroscopy study confirms the presence of two main absorption bands indicating tetrahedral and octahedral group complexes, within the spinel lattice. We also report hopping length (LA and LB), strain (ɛ) and dislocation density (ρD) of ferrite sample.

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