Journal of Synchrotron Radiation (Jul 2023)
A MHz X-ray diffraction set-up for dynamic compression experiments in the diamond anvil cell
- Rachel J. Husband,
- Cornelius Strohm,
- Karen Appel,
- Orianna B. Ball,
- Richard Briggs,
- Johannes Buchen,
- Valerio Cerantola,
- Stella Chariton,
- Amy L. Coleman,
- Hyunchae Cynn,
- Dana Dattelbaum,
- Anand Dwivedi,
- Jon H. Eggert,
- Lars Ehm,
- William J. Evans,
- Konstantin Glazyrin,
- Alexander F. Goncharov,
- Heinz Graafsma,
- Alex Howard,
- Larissa Huston,
- Trevor M. Hutchinson,
- Huijeong Hwang,
- Sony Jacob,
- Johannes Kaa,
- Jaeyong Kim,
- Minseob Kim,
- Egor Koemets,
- Zuzana Konôpková,
- Falko Langenhorst,
- Torsten Laurus,
- Xinyang Li,
- Jona Mainberger,
- Hauke Marquardt,
- Emma E. McBride,
- Christopher McGuire,
- James D. McHardy,
- Malcolm I. McMahon,
- R. Stewart McWilliams,
- Alba S. J. Méndez,
- Anshuman Mondal,
- Guillaume Morard,
- Earl F. O'Bannon,
- Christoph Otzen,
- Charles M. Pépin,
- Vitali B. Prakapenka,
- Clemens Prescher,
- Thomas R. Preston,
- Ronald Redmer,
- Michael Roeper,
- Carmen Sanchez-Valle,
- Dean Smith,
- Raymond F. Smith,
- Daniel Sneed,
- Sergio Speziale,
- Tobias Spitzbart,
- Stephan Stern,
- Blake T. Sturtevant,
- Jolanta Sztuk-Dambietz,
- Peter Talkovski,
- Nenad Velisavljevic,
- Cara Vennari,
- Zhongyan Wu,
- Choong-Shik Yoo,
- Ulf Zastrau,
- Zsolt Jenei,
- Hanns-Peter Liermann
Affiliations
- Rachel J. Husband
- Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
- Cornelius Strohm
- Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
- Karen Appel
- European XFEL, Holzkoppel 4, 22869 Schenefeld, Germany
- Orianna B. Ball
- SUPA, School of Physics and Astronomy, and Centre for Science at Extreme Conditions, The University of Edinburgh, Peter Guthrie Tait Road, Edinburgh EH9 3FD, United Kingdom
- Richard Briggs
- Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USA
- Johannes Buchen
- University of Oxford, Department of Earth Sciences, South Parks Road, Oxford OX1 3AN, United Kingdom
- Valerio Cerantola
- European XFEL, Holzkoppel 4, 22869 Schenefeld, Germany
- Stella Chariton
- The University of Chicago, Consortium for Advanced Radiation Sources, 5640 South Ellis Avenue Chicago, IL 60637, USA
- Amy L. Coleman
- Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USA
- Hyunchae Cynn
- Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USA
- Dana Dattelbaum
- Los Alamos National Laboratory, Shock and Detonation Physics (M-9), PO 1663, Los Alamos, NM 87545, USA
- Anand Dwivedi
- European XFEL, Holzkoppel 4, 22869 Schenefeld, Germany
- Jon H. Eggert
- Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USA
- Lars Ehm
- Department of Geosciences, 255 Earth and Space Sciences Building (ESS), Stony Brook, NY 11794-2100, USA
- William J. Evans
- Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USA
- Konstantin Glazyrin
- Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
- Alexander F. Goncharov
- Carnegie Science, Earth and Planets Laboratory, 5241 Broad Branch Road, NW, Washington, DC 20015, USA
- Heinz Graafsma
- Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
- Alex Howard
- Washington State University, Department of Chemistry and Institute for Shock Physics, Pullman, WA 99164, USA
- Larissa Huston
- Los Alamos National Laboratory, Shock and Detonation Physics (M-9), PO 1663, Los Alamos, NM 87545, USA
- Trevor M. Hutchinson
- Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USA
- Huijeong Hwang
- Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
- Sony Jacob
- Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USA
- Johannes Kaa
- European XFEL, Holzkoppel 4, 22869 Schenefeld, Germany
- Jaeyong Kim
- Hanyang University, Department of Physics, 17 Haengdang Dong, Seongdong gu Seoul 133-791, Republic of Korea
- Minseob Kim
- Washington State University, Department of Chemistry and Institute for Shock Physics, Pullman, WA 99164, USA
- Egor Koemets
- University of Oxford, Department of Earth Sciences, South Parks Road, Oxford OX1 3AN, United Kingdom
- Zuzana Konôpková
- European XFEL, Holzkoppel 4, 22869 Schenefeld, Germany
- Falko Langenhorst
- Institut für Geowissenschaften, Friedrich-Schiller-Universität Jena, Carl-Zeiss-Promenade 10, 07745 Jena, Germany
- Torsten Laurus
- Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
- Xinyang Li
- Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
- Jona Mainberger
- Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
- Hauke Marquardt
- University of Oxford, Department of Earth Sciences, South Parks Road, Oxford OX1 3AN, United Kingdom
- Emma E. McBride
- SLAC National Accelerator Laboratory, 2575 Sand Hill Road, Menlo Park, CA 94025, USA
- Christopher McGuire
- Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USA
- James D. McHardy
- SUPA, School of Physics and Astronomy, and Centre for Science at Extreme Conditions, The University of Edinburgh, Peter Guthrie Tait Road, Edinburgh EH9 3FD, United Kingdom
- Malcolm I. McMahon
- SUPA, School of Physics and Astronomy, and Centre for Science at Extreme Conditions, The University of Edinburgh, Peter Guthrie Tait Road, Edinburgh EH9 3FD, United Kingdom
- R. Stewart McWilliams
- SUPA, School of Physics and Astronomy, and Centre for Science at Extreme Conditions, The University of Edinburgh, Peter Guthrie Tait Road, Edinburgh EH9 3FD, United Kingdom
- Alba S. J. Méndez
- Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
- Anshuman Mondal
- Universität Münster, Institut für Mineralogie, Corrensstraße 24, 48149 Münster, Germany
- Guillaume Morard
- Univ. Grenoble Alpes, Univ. Savoie Mont Blanc, CNRS, IRD, Univ. Gustave Eiffel, ISTerre, 38000 Grenoble, France
- Earl F. O'Bannon
- Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USA
- Christoph Otzen
- Institut für Geowissenschaften, Friedrich-Schiller-Universität Jena, Carl-Zeiss-Promenade 10, 07745 Jena, Germany
- Charles M. Pépin
- CEA, DAM, DIF, 91297 Arpajon Cedex, France
- Vitali B. Prakapenka
- The University of Chicago, Consortium for Advanced Radiation Sources, 5640 South Ellis Avenue Chicago, IL 60637, USA
- Clemens Prescher
- Albert-Ludwigs University of Freiburg, Institute of Earth and Environmental Sciences, Hermann-Herder-Str. 5, D-79104 Freiburg, Germany
- Thomas R. Preston
- European XFEL, Holzkoppel 4, 22869 Schenefeld, Germany
- Ronald Redmer
- Universität Rostock, Institut für Physik, Albert-Einstein-Straße 23–24, 18059 Rostock, Germany
- Michael Roeper
- Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
- Carmen Sanchez-Valle
- Universität Münster, Institut für Mineralogie, Corrensstraße 24, 48149 Münster, Germany
- Dean Smith
- Argonne National Laboratory, High Pressure Collaborative Access Team (HPCAT), X-ray Science Division (XSD), 9700 S. Cass Avenue, Lemont, IL 60439, USA
- Raymond F. Smith
- Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USA
- Daniel Sneed
- Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USA
- Sergio Speziale
- Deutsches GeoForschungsZentrum GFZ, Telegrafenberg, 14473 Potsdam, Germany
- Tobias Spitzbart
- Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
- Stephan Stern
- Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
- Blake T. Sturtevant
- Los Alamos National Laboratory, Shock and Detonation Physics (M-9), PO 1663, Los Alamos, NM 87545, USA
- Jolanta Sztuk-Dambietz
- European XFEL, Holzkoppel 4, 22869 Schenefeld, Germany
- Peter Talkovski
- Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
- Nenad Velisavljevic
- Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USA
- Cara Vennari
- Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USA
- Zhongyan Wu
- Hanyang University, Department of Physics, 17 Haengdang Dong, Seongdong gu Seoul 133-791, Republic of Korea
- Choong-Shik Yoo
- Washington State University, Department of Chemistry and Institute for Shock Physics, Pullman, WA 99164, USA
- Ulf Zastrau
- European XFEL, Holzkoppel 4, 22869 Schenefeld, Germany
- Zsolt Jenei
- Lawrence Livermore National Laboratory, Physical and Life Science Directorate, Livermore, CA 94550, USA
- Hanns-Peter Liermann
- Deutsches Elektronen-Synchrotron DESY, Notkestr. 85, 22607 Hamburg, Germany
- DOI
- https://doi.org/10.1107/S1600577523003910
- Journal volume & issue
-
Vol. 30,
no. 4
pp. 671 – 685
Abstract
An experimental platform for dynamic diamond anvil cell (dDAC) research has been developed at the High Energy Density (HED) Instrument at the European X-ray Free Electron Laser (European XFEL). Advantage was taken of the high repetition rate of the European XFEL (up to 4.5 MHz) to collect pulse-resolved MHz X-ray diffraction data from samples as they are dynamically compressed at intermediate strain rates (≤103 s−1), where up to 352 diffraction images can be collected from a single pulse train. The set-up employs piezo-driven dDACs capable of compressing samples in ≥340 µs, compatible with the maximum length of the pulse train (550 µs). Results from rapid compression experiments on a wide range of sample systems with different X-ray scattering powers are presented. A maximum compression rate of 87 TPa s−1 was observed during the fast compression of Au, while a strain rate of ∼1100 s−1 was achieved during the rapid compression of N2 at 23 TPa s−1.
Keywords
