Metals (May 2023)

The Assessment of the Transversal Rupture Strength (TRS) and Hardness of WC-Co Specimens Made via Additive Manufacturing and Sinter-HIP

  • Ovidiu-Darius Jucan,
  • Rareş-Vasile Gădălean,
  • Horea-Florin Chicinaş,
  • Nicolae Bâlc,
  • Cătălin-Ovidiu Popa

DOI
https://doi.org/10.3390/met13061051
Journal volume & issue
Vol. 13, no. 6
p. 1051

Abstract

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This study is focused on the mechanical properties of WC-Co composites obtained via Selective Laser Sintering (SLS) using PA12 as a binder. The as-printed samples were thermally debonded and sintered, first in a vacuum, and then sinter-HIP (Hot Isostatic Pressure) at 1400 °C, using 50 bar Ar, which has led to relative densities up to 66%. Optical metallographic images show a microstructure consisting of WC, with an average grain size in the range of 1.4–2.0 µm, with isolated large grains, in a well-distributed Co matrix. The shrinkage of the samples was 43%, with no significant shape distortion. The printing direction of the samples significantly impacts the transversal rupture strength (TRS). Nevertheless, the mechanical strength was low, with a maximum of 612 MPa. SEM images of the fracture surface of TRS samples show the presence of defects that constitute the cause of the low measured values. The hardness values position the obtained composites in the medium coarse classical cemented carbides range. The results were also related to the amount of free Co after sintering, close to the initial one, as assessed by magnetic measurements, indicating a low degree of interaction with PA12 decomposition products.

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