Nanomaterials (Sep 2021)

Integration Technology for Wafer-Level LiNbO<sub>3</sub> Single-Crystal Thin Film on Silicon by Polyimide Adhesive Bonding and Chemical Mechanical Polishing

  • Wenping Geng,
  • Xiangyu Yang,
  • Gang Xue,
  • Wenhao Xu,
  • Kaixi Bi,
  • Linyu Mei,
  • Le Zhang,
  • Xiaojuan Hou,
  • Xiujian Chou

DOI
https://doi.org/10.3390/nano11102554
Journal volume & issue
Vol. 11, no. 10
p. 2554

Abstract

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An integration technology for wafer-level LiNbO3 single-crystal thin film on Si has been achieved. The optimized spin-coating speed of PI (polyimide) adhesive is 3500 rad/min. According to Fourier infrared analysis of the chemical state of the film baked under different conditions, a high-quality PI film that can be used for wafer-level bonding is obtained. A high bonding strength of 11.38 MPa is obtained by a tensile machine. The bonding interface is uniform, completed and non-porous. After the PI adhesive bonding process, the LiNbO3 single-crystal was lapped by chemical mechanical polishing. The thickness of the 100 mm diameter LiNbO3 can be decreased from 500 to 10 μm without generating serious cracks. A defect-free and tight bonding interface was confirmed by scanning electron microscopy. X-ray diffraction results show that the prepared LiNbO3 single-crystal thin film has a highly crystalline quality. Heterogeneous integration of LiNbO3 single-crystal thin film on Si is of great significance to the fabrication of MEMS devices for in-situ measurement of space-sensing signals.

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