Gold Nanoparticles Mediate Improved Detection of β-amyloid Aggregates by Fluorescence
Pedro Jara-Guajardo,
Pablo Cabrera,
Freddy Celis,
Mónica Soler,
Isadora Berlanga,
Nicole Parra-Muñoz,
Gerardo Acosta,
Fernando Albericio,
Fanny Guzman,
Marcelo Campos,
Alejandra Alvarez,
Francisco Morales-Zavala,
Marcelo J Kogan
Affiliations
Pedro Jara-Guajardo
Departamento de Química Farmacológica y Toxicológica, Facultad de Ciencias Químicas y Farmacéuticas, Universidad de Chile, Santiago 8380494, Chile
Pablo Cabrera
Departamento de Química Farmacológica y Toxicológica, Facultad de Ciencias Químicas y Farmacéuticas, Universidad de Chile, Santiago 8380494, Chile
Freddy Celis
Laboratorio de Procesos Fotónicos y Electroquímicos, Universidad de Playa Ancha, Playa Ancha 850, Valparaíso, Chile
Mónica Soler
Departamento de Ingeniería Química, Biotecnología y Materiales, Facultad de Ciencias Físicas y Matemáticas, Universidad de Chile, Beaucheff 851, Santiago 8380494, Chile
Isadora Berlanga
Departamento de Ingeniería Química, Biotecnología y Materiales, Facultad de Ciencias Físicas y Matemáticas, Universidad de Chile, Beaucheff 851, Santiago 8380494, Chile
Nicole Parra-Muñoz
Departamento de Ingeniería Química, Biotecnología y Materiales, Facultad de Ciencias Físicas y Matemáticas, Universidad de Chile, Beaucheff 851, Santiago 8380494, Chile
Gerardo Acosta
CIBER-BBN, Networking Centre on Bioengineering, Biomaterials and Nanomedicine & Department of Organic Chemistry, Marti i Franques 1-11, University of Barcelona (UB), 08028 Barcelona, Spain
Fernando Albericio
CIBER-BBN, Networking Centre on Bioengineering, Biomaterials and Nanomedicine & Department of Organic Chemistry, Marti i Franques 1-11, University of Barcelona (UB), 08028 Barcelona, Spain
Fanny Guzman
Núcleo de Biotecnología Curauma (NBC), Pontificia Universidad Católica de Valparaíso, Valparaíso 2460355, Chile
Marcelo Campos
Department of Chemistry, Faculty of Sciences, University of Chile, POBox 653, Santiago 8380494, Chile
Alejandra Alvarez
Facultad de Ciencias Biológicas, Pontificia Universidad Católica de Chile, Alameda 340, Santiago 8331010, Chile
Francisco Morales-Zavala
Departamento de Química Farmacológica y Toxicológica, Facultad de Ciencias Químicas y Farmacéuticas, Universidad de Chile, Santiago 8380494, Chile
Marcelo J Kogan
Departamento de Química Farmacológica y Toxicológica, Facultad de Ciencias Químicas y Farmacéuticas, Universidad de Chile, Santiago 8380494, Chile
The early detection of the amyloid beta peptide aggregates involved in Alzheimer’s disease is crucial to test new potential treatments. In this research, we improved the detection of amyloid beta peptide aggregates in vitro and ex vivo by fluorescence combining the use of CRANAD-2 and gold nanorods (GNRs) by the surface enhancement fluorescence effect. We synthetized GNRs and modified their surface with HS-PEG-OMe and HS-PEG-COOH and functionalized them with the D1 peptide, which has the capability to selectively bind to amyloid beta peptide. For an in vitro detection of amyloid beta peptide, we co-incubated amyloid beta peptide aggregates with the probe CRANAD-2 and GNR-PEG-D1 observing an increase in the intensity of the fluorescence signal attributed to surface enhancement fluorescence. Furthermore, the surface enhancement fluorescence effect was observed in brain slices of transgenic mice with Alzheimer´s disease co-incubated with CRANAD-2 and GNR-PEG-D1. An increase in the fluorescence signal was observed allowing the detection of aggregates that cannot be detected with the single use of CRANAD-2. Gold nanoparticles allowed an improvement in the detection of the amyloid aggregated by fluorescence in vitro and ex vivo.