Physical Review Research (Jul 2020)

X-ray coherent diffraction imaging with an objective lens: Towards three-dimensional mapping of thick polycrystals

  • A. F. Pedersen,
  • V. Chamard,
  • C. Detlefs,
  • T. Zhou,
  • D. Carbone,
  • H. F. Poulsen

DOI
https://doi.org/10.1103/PhysRevResearch.2.033031
Journal volume & issue
Vol. 2, no. 3
p. 033031

Abstract

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We demonstrate an x-ray coherent imaging method that combines high spatial resolution with the ability to map grains within thick polycrystalline specimens. An x-ray objective serves to isolate an embedded grain. Iterative oversampling routines and Fourier synthesis are used to reconstruct the shape and strain field from the far-field intensity pattern. In a demonstration experiment a ∼500-nm Pt grain embedded in a polycrystalline Pt matrix is mapped in three dimensions without compromising the spatial resolution. No information on the pupil function of the lens is required and lens aberrations are not critical.