Eurasian Chemico-Technological Journal (Dec 2011)

Determination of Calibration Characteristics of X-Ray Fluorescent Analysis of Rhenium

  • A. V. Troeglazova,
  • E. V. Zlobina,
  • A. Yu. Sokolov,
  • A. K. Zhangalieva

DOI
https://doi.org/10.18321/ectj214
Journal volume & issue
Vol. 13, no. 3-4
pp. 247 – 251

Abstract

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Extraction concentration of rhenium by a melt of tetraoctylammonium bromide in paraffin was used with the aim of preparation of calibration samples for roentgen fluorescent analysis. The calibration characteristics of the roentgen fluorescent analysis of rhenium is established, its linearity is evaluated, a limit of detection and a limit of quantification (determination) of rhenium are calculated. The maximal value of the relative total standard uncertainty of the calibration characteristic does not exceed 1.45%. ristic does not exceed 1.45%.