From dislocation nucleation to dislocation multiplication in ceramic nanoparticle

Abstract

Magnesium oxide nanocubes are compressed along the [001] direction in situ in the transmission electron microscope. Incipient plasticity in the smaller samples is characterized by the nucleation of few $ \raise.5ex\hbox{$\scriptstyle 1$}\kern-.1em/\kern-.15em\lower.25ex\hbox{$\scriptstyle 2$} {\lt}110{\gt} \{{110} \} $ dislocations while a larger number of line defects is observed in larger nanocubes. Yield and flow stresses scattered stochastically above a minimum value varying as the inverse of the sample size. The upper bound is given by the reduced number of dislocation sources. Such size-dependent behaviour is justified by a detailed statistical analysis and is fully explained by the deformation mechanism.

Keywords

• in situ
• tem
• compression
• dislocation
• mgo