A Modified-One Pot Synthesis of Diaminoglyoxime

Ali Kakanejadifard; S. Morteza Farnia; Golamreza Najafi

Iranian Journal of Chemistry & Chemical Engineering (Apr 2004)

A Modified-One Pot Synthesis of Diaminoglyoxime

Ali Kakanejadifard,
S. Morteza Farnia,
Golamreza Najafi

Affiliations

Ali Kakanejadifard: Department of Chemistry, Faculty of Science, University of Lorestan, P.O. Box 465, Khoramabad, I. R. IRAN
S. Morteza Farnia: Department of Chemistry, Faculty of Science, Tehran University, Tehran, I. R. IRAN.
Golamreza Najafi: Department of Chemistry, Faculty of Science, Tehran University, Tehran, I. R. IRAN

Journal volume & issue: Vol. 23, no. 1
pp. 117 – 118

Abstract

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The one pot reaction of glyoxal and hydroxylamine hydrochloride in aqueous sodium hydroxide was found to be a safe and inexpensive method for the preparation of diaminoglyoxime. By increasing stoichiometric ratio of the hydroxylamine hydrochloride and decreasing the solvent volume, the product yield increased considerably (~ 70%).

Published in Iranian Journal of Chemistry & Chemical Engineering

ISSN: 1021-9986 (Print)
Publisher: Iranian Institute of Research and Development in Chemical Industries (IRDCI)-ACECR
Country of publisher: Iran, Islamic Republic of
LCC subjects: Technology: Chemical technology: Chemical engineering; Science: Chemistry
Website: http://www.ijcce.ac.ir

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