Química Nova (Jan 2012)

Caracterização de resíduo sólido formado em biodiesel de sebo bovino

  • Valter José Fernandes Júnior,
  • Antonio de Sousa Araujo,
  • Fábio da Silva Vinhado,
  • Paulo Roberto Pivesso

DOI
https://doi.org/10.1590/s0100-40422012001000002
Journal volume & issue
Vol. 35, no. 10
pp. 1901 – 1906

Abstract

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The nature of the solid residue formed in beef tallow biodiesel from two commercial producers in Brazil was determined by comparative analytical techniques, namely, gas chromatography with flame ionization detector (GC-FID) and thermogravimetry (TG). Pure monopalmitin and monostearin were used as reference standards for both methodologies. Analyses were carried out before and after filtration of the solids formed, which allowed the observation that the formation of precipitate reduced the levels of monoglycerides in the beef tallow biodiesel. The chromatographic and thermogravimetric results confirmed the nature of the residue as saturated monoglycerides, predominantly monostearin and monopalmitin.

Keywords