Carbon: Science and Technology (Mar 2013)

Effect of temperature on the crystallite size of Lanthanum Cerium Oxide (La2Ce2O7) and its optical properties

  • Hozefa Tinwala,
  • D. C. Shah ,
  • Jyoti Menghani

Journal volume & issue
Vol. 5, no. 1
pp. 225 – 230

Abstract

Read online

The effect of the calcination process on the crystallite size and optical properties of Lanthanum Cerium Oxide (La2Ce2O7) nanopowders synthesized using co-precipitation process were reported. X-ray diffraction analysis revealed that the synthesized nanopowders calcined at various temperatures have cubic fluorite phase. Thermal Gravimetric Analysis (TGA), X-ray Diffraction (XRD), Energy Dispersive Spectroscopy (EDS), Transmission Electron Microscopy (TEM), Laser Raman Spectroscopy, and UVvisible spectroscopy were utilized to characterize phase structure and morphology of the products.

Keywords