Química Nova (Jan 2013)

Câmara de volatilização: uma alternativa para avaliação da eficiência de amostragem de α- e <FONT FACE=Symbol>β</FONT>-endossulfam em fase gasosa

  • João L. Freixo,
  • Diego B. da Silva,
  • Eliana F. G. de C. Dores,
  • Ricardo D. Villa

DOI
https://doi.org/10.1590/S0100-40422013000700019
Journal volume & issue
Vol. 36, no. 7
pp. 1038 – 1043

Abstract

Read online

The efficiency of XAD®-2 resin in sampling the pesticides α and β-endosulfan from air contaminated in the laboratory was evaluated. Sampling efficiency ranged from 87 to 108% for α-endosulfan and from 71 to 84% for β-endosulfan with relative standard deviation lower than 19%. The pesticides were not detected in the second section of the cartridge showing the good retention capacity of XAD®-2 for these analytes. Method quantification limits were 0.32 and 0.34 µg m-3 for α and β-endosulfan, respectively. These results suggest that the proposed method may be useful for evaluating occupational exposure to these compounds.

Keywords