Ceramics (Nov 2024)

Effect of High Heat Flux of Helium and Hydrogen Plasma Jet on the Material Properties of Piezoelectric PZT-Ceramics

  • Galina Yu. Sotnikova,
  • Alexander V. Ankudinov,
  • Alexander V. Voronin,
  • Gennady A. Gavrilov,
  • Alexey L. Glazov,
  • Valery Yu. Goryainov,
  • Nina V. Zaitseva,
  • Alexey V. Nashchekin,
  • Rostislav S. Passet,
  • Alexander A. Vorob’ev,
  • Andrey V. Sotnikov

DOI
https://doi.org/10.3390/ceramics7040108
Journal volume & issue
Vol. 7, no. 4
pp. 1695 – 1710

Abstract

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A set of experimental and measurement techniques to study the influence of a plasma jet on the main material parameters of piezoelectric ceramics has been presented. A series of plasma experiments has been carried out using a pulsed plasma jet system. It allows of a metered-dose exposure to plasma of different composition and fluence with a constant particle flux density of 1021/m2, energy flux density of 0.1 MJ/m2 and average particle energy of 100–200 eV in a pulse duration of 15 μs. The study of the effects that a repeated exposure to an extreme heat flux of helium and hydrogen plasmas has on the near-surface layer structure and basic material parameters of mass-produced piezoelectric ceramic samples has been presented. The main result of the research is an experimental confirmation of the surface micro-structuring starting after just a few cycles of plasma exposure while only a slight decrease of the main material parameters as well as the preservation of polarization has been observed for two types of different compositions of PZT-ceramics. A further increase in the number of exposure pulses leads to practically no change of main material parameters of both ceramics, even showing a tendency for recovery instead.

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