Archives of Metallurgy and Materials (Dec 2018)

Structure, Morphology and Electrical Properties of CaTiO3 Ceramics Synthesized by the Solid-State Reaction Method

  • E. Rocha-Rangel,
  • J. López-Hernández,
  • J.A. Castillo-Martínez,
  • J.J. Osorio-Ramos,
  • C.A. Calles-Arriaga,
  • I. Estrada-Guel,
  • R. Martínez-Sánchez

DOI
https://doi.org/10.24425/amm.2018.125101
Journal volume & issue
Vol. vol. 63, no. No 4
pp. 1749 – 1753

Abstract

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In this paper, explain the preparation of CaTiO3 ceramics synthesized by the solid-state reaction method. Calcium carbonate and titanium dioxide were high energy mixed in stoichiometric amounts, and the obtained mixture was calcined at different temperatures (800, 900, 1000 and 1300ºC) for 2 h. The obtained samples were characterized by measurement of particle size, Energy Dispersive X-Ray (EDX) Analysis; differential thermal analysis, X-ray diffraction and SEM images. XRD patterns indicated that CaTiO3 ceramics with the structure of perovskite is obtained from calcined powders at 1,300°C for 2 h. SEM images show the formation of a very fine and homogeneous morphology. The measured values of electrical resistivity were within the typical range of insulating materials and approach values corresponding to insulating ceramics.

Keywords