Acta Crystallographica Section E: Crystallographic Communications (Feb 2024)

Synthesis and crystal structure of N1,N2-dimethylethanedihydrazide

  • Yurii S. Bibik,
  • Dmytro M. Khomenko,
  • Roman O. Doroshchuk,
  • Ilona V. Raspertova,
  • Alexandra Bargan,
  • Rostyslav D. Lampeka

DOI
https://doi.org/10.1107/S2056989024000239
Journal volume & issue
Vol. 80, no. 2
pp. 148 – 151

Abstract

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The title compound, N1,N2-dimethylethanedihydrazide, C4H10N4O2, was obtained by the methylation of oxalyl dihydrazide protected with phthalimide. The molecule is essentially non-planar with a dihedral angle between the two planar hydrazide fragments of 86.5 (2)°. This geometry contributes to the formation of a multi-contact three-dimensional supramolecular network via C—H...O, N—H...O and N—H...N hydrogen bonds.

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