Zeitschrift für Kristallographie - New Crystal Structures (Mar 2013)

Crystal structure of μ3-fluoro-tri-μ2-fluoro-tris(tetramethylethylenediamine nickel(II)) fluoride trihydrate, [Ni3(tmen)3F5]+·F–·3H2O, C18H54F6N6Ni3O3

  • Ishikawa Yuki,
  • Miyamoto Keiko,
  • Horn Ernst

DOI
https://doi.org/10.1524/ncrs.2013.0019
Journal volume & issue
Vol. 228, no. 1
pp. 126 – 128

Abstract

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C18H54F6N6O3Ni3, triclinic, P1̄ (no. 2), a = 8.6908(7) Å, b = 13.717(1) Å, c = 14.281(1) Å, α = 72.997(1)°, β = 89.459(1)°, γ = 75.718(1)°, V = 1574.1(2) Å3, Z = 2, Rgt(F) = 0.0355, wRref(F2) = 0.0433, T = 273,2 K.