Effect of Pre-Added HfO₂ Inclusions on Carbide Morphology and Deformation Behavior in DZ125 Nickel-Based Superalloy

Abstract

Inclusions are important phases affecting material properties in complicated ways. In this paper, a quantitative study of the addition of HfO2 inclusions to DZ125 nickel-based superalloys was performed. Experimental results showed that the introduction of HfO2 inclusions caused a loss of strength and ductility. The carbide morphology also changed significantly from skeletal-shaped to block-shaped, resulting in a remarkable discrepancy in the fracture behavior under quasi-in-situ tensile testing. The SEM dynamic observations showed that cracks were initiated from the skeletal carbides and almost failed to propagate into the matrix. In contrast, the damage behavior of block-shaped carbides also involved internal cracking but with a tendency to form interconnected microcracks during propagation. A crystal plasticity finite element model (CPFEM) method was further developed to study the stress/strain behavior during the deformation process, considering the crystal orientations and microstructure morphologies from the EBSD data. Those elastoplastic parameters were determined through nanoindentation experiments. Simulation results verified that blocky carbides produced a pronounced strain concentration at the interface of the carbides and matrix, thereby increasing the tendency of crack formation. This paper provides a fundamental understanding of the role of inclusions in material recycling applications.

Keywords

• inclusions
• carbide
• nickel-based superalloy
• deformed behavior
• CPFEM