Acta Crystallographica Section E (Dec 2008)

N-(2,4-Dinitrophenyl)-N′-[nitro(phenyl)methylene]hydrazine

  • Chunlan Yuan

DOI
https://doi.org/10.1107/S1600536808036179
Journal volume & issue
Vol. 64, no. 12
pp. o2297 – o2297

Abstract

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The title compound, C13H9N5O6, contains three nitro groups. It is prepared by the reaction of benzaldehyde 2,4-dinitrophenylhydrazone with nitric oxide at ambient temperature. The imine group is nearly coplanar with the (2,4-dinitrophenyl)hydrazine unit. The second benzene ring and the third nitro group are twisted away from this plane, with dihedral angles of 48.5 (3) and 15.2 (3)°, respectively. Weak intramolecular N—H...O interactions are observed.