Acta Crystallographica Section E (May 2009)

2-(3-Oxo-1,3-dihydroisobenzofuran-1-yl)phthalazin-1(2H)-one

  • Hong Deng,
  • Guo Peng,
  • Yu-Jun Wu,
  • You-Lei Zhang

DOI
https://doi.org/10.1107/S1600536809011970
Journal volume & issue
Vol. 65, no. 5
pp. o974 – o974

Abstract

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The reaction of 2-carboxybenzaldehyde and hydrazine hydrate unexpectedly yielded the title compound, C16H10N2O3, which comprises one phthalide ring, one phthalazine system and a chiral centre. The phthalide unit is almost perpendicular to the phthalazine system, forming a dihedral angle of 87.1 (3)°. The packing is governed by weak C—H...O hydrogen-bonding interactions, forming layers parallel to the ab plane.