A Direct Method for the Efficient Synthesis of Hydroxyalkyl-Containing Azoxybenzenes

Ekaterina S. Spesivaya; Ida A. Lupanova; Dzhamilya N. Konshina; Valery V. Konshin

doi:10.3390/M1384

Molbank (Jun 2022)

A Direct Method for the Efficient Synthesis of Hydroxyalkyl-Containing Azoxybenzenes

Ekaterina S. Spesivaya,
Ida A. Lupanova,
Dzhamilya N. Konshina,
Valery V. Konshin

Affiliations

Ekaterina S. Spesivaya: Department of Chemistry and High Technology, Kuban State University, Stavropolskayast 149, 350040 Krasnodar, Russia
Ida A. Lupanova: Department of Chemistry and High Technology, Kuban State University, Stavropolskayast 149, 350040 Krasnodar, Russia
Dzhamilya N. Konshina: Department of Chemistry and High Technology, Kuban State University, Stavropolskayast 149, 350040 Krasnodar, Russia
Valery V. Konshin: Department of Chemistry and High Technology, Kuban State University, Stavropolskayast 149, 350040 Krasnodar, Russia

DOI: https://doi.org/10.3390/M1384
Journal volume & issue: Vol. 2022, no. 2
p. M1384

Abstract

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Reaction of nitrobenzyl alcohol with glucose (200 mol%) in the presence of NaOH in water-ethanol medium gave 1,2-bis(4-(hydroxymethyl)phenyl)diazene oxide, 1,2-bis(2-(hydroxymethyl)phenyl)diazene oxide and 1,2-bis(4-(1-hydroxyethyl)phenyl)diazene oxide in 76%, 76% and 72% yields, respectively.

Published in Molbank

ISSN: 1422-8599 (Online)
Publisher: MDPI AG
Country of publisher: Switzerland
LCC subjects: Science: Chemistry: Inorganic chemistry
Website: https://www.mdpi.com/journal/molbank

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Abstract

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