Journal of Chemistry (Jan 2019)

A Novel Approach for Fabricating LaMnO3 Thin Films Using Combined Microwave Combustion and Pulsed Electron Deposition Techniques

  • Thi Ha Tran,
  • Thi Trung Anh Tang,
  • Nguyen Hai Pham,
  • Thanh Cong Bach,
  • Cong Doanh Sai,
  • Quang Hoa Nguyen,
  • Van Vu Le,
  • Hoang Nam Nguyen,
  • Quoc Khoa Doan,
  • Trong Tam Nguyen,
  • Viet Bau Le,
  • Khac Hieu Ho,
  • Viet Tuyen Nguyen

DOI
https://doi.org/10.1155/2019/3568185
Journal volume & issue
Vol. 2019

Abstract

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LaMnO3 (LMO) nanopowder was synthesized by the microwave combustion method using glycine and nitrate salts of La and Mn as precursors. The as-prepared LMO powder was pressed at high pressure and annealed at 1000°C for 8 hours to make a target for thin film deposition. The structural and elemental analysis was obtained by X-ray diffraction (XRD) and energy dispersive X-ray spectroscopy (EDS). Thin films of LMO were fabricated using pulsed electron deposition (PED) at room temperature. The effects of discharge voltage and oxygen/argon flux ratio on the produced thin films were studied. The study shows that stoichiometry and structure of the target was preserved well in the thin films prepared with a discharge voltage from 14 to 15 kV, while the oxygen/nitrogen flux ratio did not show a clear effect on the quality of thin films.