Acta Crystallographica Section E (Nov 2010)
5-[(E)-Benzylidene]-2-hydroxy-10-methyl-8-phenyl-3,10-diazahexacyclo[10.7.1.13,7.02,11.07,11.016,20]henicosa-1(19),12(20),13,15,17-pentaen-6-one ethanol 0.25-solvate 0.6-hydrate
Abstract
In the title compound, C33H28N2O2·0.25C2H6O·0.6H2O, the piperidone ring adopts a chair conformation and the pyrrolidine ring adopts an envelope conformation. The dihedral angle between the two phenyl rings is 70.83 (16)°. One of the N atoms of the organic molecule is disordered over two positions in a 0.52 (4):0.48 (4) ratio and the two solvent molecules are partially occupied and show high displacement parameters. In the crystal, molecules are connected by intermolecular O—H...O and C—H...O hydrogen bonds, forming a three-dimensional network.