Preparation of microcrystalline cellulose from Rabdosia rubescens residue and study on its membrane properties

Abstract

Abstract Microcrystalline cellulose (MCC) was prepared easily from Rabdosia rubescens residue to realize the efficient utilization of waste resources. The yield was about 95.03% under the optimal conditions. Then, MCC membrane was prepared by phase transformation method and its structure and mechanical properties were studied systemically. The results showed the cellulose crystal structure changed from type I to type II in the process of forming membrane, and the thermal stability decreased simultaneously. The content of MCC in casting solution has great influence on the mechanical properties of membranes. The higher the content of MCC, the better the comprehensive mechanical properties of the membranes is. When MCC content is 9%, the tensile strength and elongation at break can reach 8.38 MPa and 26.72%, which is better than traditional cellulose membranes. Finally, the separation properties were studied by separation BSA from water. The results showed that the rejection rate and water flux changed positively and negatively with the change of MCC content. When the content was 5%, the membrane demonstrated the best comprehensive performance, its rejection for BSA was 37.23 g/(m2 h), the corresponding rejection rate and water flux were 88.87% and 41.89 L/(m2 h) respectively.