Fabrication of Silicon Carbide Fiber-Reinforced Silicon Carbide Matrix Composites Using Binder Jetting Additive Manufacturing from Irregularly-Shaped and Spherical Powders

Abstract

In this paper, silicon carbide fiber-reinforced silicon carbide (SiCf/SiC) composites were fabricated using binder jetting additive manufacturing followed by polymer infiltration and pyrolysis. Spherical SiC powders were produced using milling, spray drying, and thermal plasma treatment, and were characterized using SEM and XRD methods. Irregularly shaped and spherical SiC powders were used to obtain SiCf/SiC blends for the application in binder jetting. The effect of SiC powder shape on densification behavior, microstructure, and mechanical properties of binder jetted SiCf/SiC composites was evaluated. The highest density of 2.52 g/cm3 was obtained after six polymer infiltration and pyrolysis cycles. The microstructure and mechanical properties of the fabricated SiCf/SiC composites were characterized. Using the spherical SiC powder resulted in higher fracture toughness and hardness, but lower flexural strength compared to the irregularly shaped powder. It was shown that it is feasible to fabricate dense SiCf/SiC composites using binder jetting followed by polymer infiltration and pyrolysis.

Keywords

• additive manufacturing
• binder jetting
• silicon carbide
• spray drying
• pyrolysis