Acta Crystallographica Section E (Mar 2012)

Diethyl 4,4′-(3,6-dioxaoctane-1,8-diyldioxy)dibenzoate

  • Jingjie Fan,
  • Gang Lai,
  • Zhen Ma,
  • Haisha Qin

DOI
https://doi.org/10.1107/S1600536812004874
Journal volume & issue
Vol. 68, no. 3
pp. o714 – o714

Abstract

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The title compound, C24H30O8, was obtained by reaction of ethyl 4-hydroxybenzoate with 1,2-dichloroethane. The molecule occupies a crystallographic inversion center, with its central ethylene bridge in an anti conformation. The other ethylene bridge has a gauche conformation, with the corresponding O—C—C—O torsion angle being 74.2 (1)°. The benzene rings are almost coplanar with the adjacent ethoxycarbonyl groups, with an r.m.s. deviation of 0.078 Å.