The influence of the deposition parameters on the porosity of thin alumina films on steel

Abstract

The influence of the deposition parameters on the porosity of thin alumina films electrophoretically deposited on steel from aqueous suspensions was investigated. The effects of the applied voltage, deposition time, suspension temperature and the solid content of the aqueous suspension on the porosity of the obtained alumina films have been determined using optical microscopy coupled with image analysis. It was shown that the lowest film porosity was obtained from a suspension containing 20 wt.% alumina powder at the lowest applied voltage (30 V), for a longer deposition time (10 min) using a suspension temperature of 30 ºC. This behavior can be explained by the smaller amount of hydrogen evolved on the cathode during the electrophoretic deposition process.

Keywords

• alumina
• cataphoretic deposition
• deposition parameters
• image analysis
• porosity