Acta Crystallographica Section E (Aug 2012)

Diethyl 4-(4-acetamidophenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate

  • Yiliang Zhao,
  • David E. Hibbs,
  • Paul W. Groundwater,
  • Abram Wassef

DOI
https://doi.org/10.1107/S160053681202750X
Journal volume & issue
Vol. 68, no. 8
pp. o2536 – o2536

Abstract

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The title compound, C21H26N2O5, was unexpectedly obtained as a by-product in the reaction of ethyl acetoacetate, 4-acetamidobenzaldehyde and urea under microwave irradiation. The dihydropyridine ring assumes a flattened boat conformation. Intermolecular N—H...O and weak C—H...O hydrogen bonding occurs in the crystal.